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GLYCEROL Extra Pure Confirming to IP 1,2,3-Propanetriol; Glycerin

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Description

Article No. 00155 Grade Extra Pure
Purity 98% CAS No. 56-81-5
Molecular Formula C3H8O3 Molecular Weight 92.09
H.S. Code 2905.4500 Shelf Life 60 Months

Physical Properties

Physical state at 20 °C Liquid Colour Clear colorless
Odour Odorless pH value 5.5 – 8
Melting point/ Freezing point [°C] 20 °C Auto-ignition temperature [°C] 370°C
Flash point [°C] 160 °C Boiling point [°C] 182 °C
Vapour pressure mm/Hg 0.0033 mm Hg at 50 °C Vapour density 3.18
Density [g/cm3] 1.25 Solubility in water [% weight] Soluble in water
Explosion limits -lower [%] 0.90%

Specifications

Appearance A clear, colourless or almost colourless, syrupy liquid; hygroscopic Solubility Miscible with water and with ethanol (95%), slightly soluble in acetone, practically insoluble in ether and in fixed oils and volatile oils.
Assay (on anhydrous basis) 98.0-101.0% Identifications –
Identification ‘A’ ( by IR) The absorption maxima in the spectrum obtained with the sample corresponds in position & relative intensity to those in the spectrum obtained with Glycerin reference standard / working standard or with the reference spectrum of Glycerin Identification ‘B’ Refractive index – 1.470 to 1.475
Identification ‘C’ Relative density – 1.258 to 1.268 Appearance of solution Solution A is clear, Solution is colourless (10 mL of solution A–> 25 mL with water)
Acidity or alkalinity Solution is colourless and not more than 0.2 mL of 0.1 M sodium hydroxide is required to produce a pink colour Chlorides Max 0.0025%
Aldehydes Max 0.001% Ester Not less than 8.0 mL of 0.1 M hydrochloric acid is required to decolourise the solution
Halogenated compounds Max 0.0035% Ethlylene glycol, diethylene glycol and related substances –
Ethylene glycol (GC) Max 0.1% Diethylene glycol (GC) Max 0.1%
Any other secondary impurity Max 0.1% Sum of all impurities Max 1.0%
Sugars The solution is clear blue. The solution remains blue and no precipitate is formed on further heating for 5mins. Heavy metals Max 0.0005%
Sulphated ash Max 0.01% Water Max 2.0%
Revision Date: 16-May-2025

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